FACILITIES AND EQUIPMENT
Lasers | Microscopes | Ultrahigh Vacuum Chambers
Electrochemical | Microanalyzer | Ellipsometry
Laboratory Facilities
Materials Research Facility (MRF) | Department and University Facilities
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ULTRAFAST LASERS

Femtosecond Ti-Sapphire
Regenerative Amplifier.
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- Picosecond/Femtosecond Ti:Sapphire Regenerative Amplifier (BMI/Coherent) 1 kHz, 0.8 mJ used to pump Infrared Optical Parametric Amplifier (OPA) 0.1-4 psec. 1.1 -3µm, > 10µJ, for Linear and Nonlinear (SHG, SFG) Optical Spectroscopy and Dynamics experiments.
- Nanosecond Nd.YLF. 527 nm, 1054 nm, 10 mJ, single shot - 5 kHz.
- Ultrashort (<25 fs) Ti:Sapphire Oscillator, tunable from 725-930 nm (< 100 fs) and harmonics, for Linear and Nonlinear (SHG, SFG) Optical Spectroscopy and Dynamics experiments.
- Femtosecond Ti:Sapphire Regenerative Amplifier (Quantronix) 1 kHz, 3.5 mJ used to pump Infrared Optical Parametric Amplifier (OPA) 1.1 -5µm > 30µJ, 5 -15µm > 30µJ, 1 kHz, for Linear and Nonlinear (SHG, SFG) Optical Spectroscopy and Dynamics experiments.
- Optics, photon detection equipment (APD, CCD, IR detectors), spectrographs, data acquisition and analysis.
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SCANNING TUNNELING/
ATOMIC FORCE MICROSCOPES

Molecular Imaging
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ULTRAHIGH
VACUUM CHAMBERS

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CHI 600C Electrochemical
Workstation

Measurement scales:
Potential range:±10 V
Current range: 0.1 A ~ pA
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Techniques included:
- Cyclic Voltammetry
- Chronoamperometry
- Chronocoulometry
- Differential Pulse Voltammetry
- Normal Pulse Voltammetry
- Square Wave Voltammetry
- Amperometric i-t Curve
- Differential Pulse Amperometry
- Double Differential Pulse Amperometry
- Open Circuit Potential-time
- Electrochemical Potentiostat, Bipotentiostat and Galvanostat.
- Spectro-electrochemical cells.
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Princeton Potentiostat
Model 273A

Measurement scales:
Potential range:±10 V
Current range: 1 A ~ 100 nA
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Techniques included:
- Cyclic Voltammetry
- Chronoamperometry
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Omni-101
Microprocessor-Controlled
Potentiostat

Measurement scales:
Potential range:
Current range: 0.1 A ~ 100 nA
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Techniques included:
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Electron Probe, X-Ray
Microanalyzer
(JEOL, JXA-733)

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PHE101M Multi-Wavelength
Ellipsometer

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Techniques included:
- Measure the refractive index, n
- Measure the extinction coefficient, k
- Measure the thickness of single and multi-layer films, d
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LABRITORY FACILITIES: PHYSICAL SPACE
- Renovated Laser Laboratory space (Laser lab >100 m2) provides temperature, humidity and dust control for state-of-the-art laser facility.
- Renovated microscopy laboratory provides temperature, humidity and dust control for state-of-the-art microscopy (AFM, STM).
- Renovated wet chemistry laboratories with Nanopure water supplies.
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MATERIALS RESEARCH FACILITY (MRF) *New
The Materials Research Facility provides a centralized location for analytical instrumentation to support faculty research efforts in the College of Science and Technology. Located in Beury Hall, this facility houses three X-Ray Diffractometers, Microprobe, TEM and Raman Mass Spectrometer.
Instrumentation
XRD Bruker Apex II
DUO |
XRD Bruker D8
Discover |
XRD Rigaku |
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| JEOL JEM-1400 TEM |
JEOL 733 Electron
Microscope |
Jasco Ventuno Raman
Spectrometer |
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DEPARTMENTAL & UNIVERSITY FACILITIES
The equipment in the Department is generally available for use by all graduate students and faculty. Usually, it is maintained by a particular research group or one of the Departmental Technicians. The operation and care of the equipment is considered integral to the education of graduate students.
- GE 500 MHz NMR (multinuclear), 2D, variable temperature and Sun workstation for all nuclei.
- QE 300 MHz NMR, 2D, variable temperature for proton and carbon.
- Bruker WM-400 MHz NMR (quad probe), 2D, variable temperature.
- Varian 60 MHz for proton and fluorine.
2. Infrared Spectrophotometers
- Digilab FTS-40 FT-IR
- Nicolet 670
- Nicolet 20SX FT-IR variable temperature.
- Mattson Cygnus 100 FT-IR with mid, near and far IR optics
- Mattson 4020 and 4040 FT-IT spectrometers for routine midrange use (3)
3. Mass Spectrometers
- Hewlett-Packard 6890 GC-MS
- Hewlett-Packard 5995c GC-MS
4. Ultraviolet-Near IRĀ Spectrometers
- Hewlett-Packard 8450 (UV/VIS)
- Perkin Elmer 330 variable temperature with P-E 3600 Data Station (UV/VIS)
- Perkin Elmer P4 (UV/VIS)
- Jasco V570 (UV-VIS-NIR)
5. Raman Spectrometers
6. Fluorescence Spectrometers
- Molecular Fluorescence Spectrometer MPF66
- Jobin Yvon Fluoromax2
- Jasco FP-750
- PTI Fluorescence Spectrometer
7. Gas Chromatographs
- Buck Scientific 910 (polar column)
- Buck Scientific 910 (nonpolar column)
8. Atomic Absorption/Emission Spectrophotometers
- Buck Scientific Atomic Absorption/Emission Spectrophotometer (2) Model 200-A
9. Other Equipment
- Bruker EMX-200R Electron Spin Resonance Spectrometer variable temperature (10K-600K), field frequency controller, programmable gaussmeter and IBM 9000 computer system.
- Enraf Nonius CAD-4 Single Crystal X-ray Diffractometer with variable temperature capabilities.
- Thermal Gravimetric Analyzer/Differential Scanning Calorimeter
- Instron model 1122 Mechanical Tester, computer controlled.
10. Ultrafast Lasers
- In the Mid-Atlantic region, the department has one of the largest collections of ultrafast lasers, based on Ti:sapphire Oscillators and Regenerative Amplifiers, as well as Optical Parametric Amplifiers. These laser are used in CAPR and the Borguet, Dai, Levis, and Stanley groups.
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